MSE 2022
Lecture
27.09.2022
Improved work hardening capability and ductility of an additively manufactured and deformed Al-Mn-Mg-Sc-Zr alloy
DS

Dr. Daniel Schliephake

Karlsruher Institut für Technologie (KIT)

Schliephake, D. (Speaker)¹; Bayoumy, D.²; Chen, H.¹; Eggeler, Y.M.¹; Freudenberger, J.³; Huang, A.²; Kauffmann, A.¹; Lopes, C.¹
¹Karlsruhe Institute of Technology (KIT); ²Monash University, Clayton (Australia); ³Leibnitz Institute for Solid State and Materials Research Dresden (IFW Dresden)
Vorschau
19 Min. Untertitel (CC)

Laser powder bed fusion (LPBF) exhibits enormous benefits for precipitation-strengthening Al alloys by significant supersaturation and the formation very fine microstructures during manufacturing. This has led to the development of several new alloys mainly containing Sc and Zr to form L12 precipitates and Mg and Mn to further increase solid solution strengthening [1,2,3]. The L12 precipitates exhibit exceptional thermal stability and provide excellent creep resistant of these alloys at 250 °C [4]. In this work, we investigate the precipitation behavior and resulting properties of an Al-Mn-Mg-Sc-Zr alloy after introducing additional vacancies and dislocations by cold working and how these additional defects influence the thermal stability of the precipitates. For this, the LPBF processed alloy was swaged at room temperature to a true strain of 2.5. Compared to the LPBF alloy, swaging results in a refinement of the microstructure by one order of magnitude and an increased hardness and ultimate tensile strength (UTS of 705 vs. 430 MPa) which is mainly attributed to the finer microstructure in the swaged alloy. By annealing, a higher peak-aging hardness and UTS of the swaged alloy at a lower peak-aging temperature in the swaged was obtained (UTS of 720 MPa vs. 570 MPa at 300 °C). Significant improvement of ductility of the swaged alloy is obtained for intermediate annealing between 300 to 400 °C while strength is only moderately affected (e.g. UTS of 590 MPa at 2 % strain to failure). This significant improvement of aging kinetics and work hardening capability is discussed alongside intense microstructural characterization of the heterogeneous grain structure and precipitate distribution.

Keywords: Al-Sc alloy, additive manufacturing, cold working, age-hardening behavior.

References:
[1] A.B. Spierings et al., SLM-processed Sc- and Zr- modified Al-Mg alloy: Mechanical properties and microstructural effects of heat treatment, Mater. Sci. Eng. A 701, 2017, 264-273.
[2] Q. Jia et al., Precipitation kinetics, microstructure evolution and mechanical behavior of a developed Al–Mn–Sc alloy fabricated by selective laser melting, Acta Mater. 193, 2020, 239-251.
[3] S. Griffiths et al., Coarsening- and creep resistance of precipitation-strengthened Al-Mg-Zr alloys processed by selective laser melting, Acta Mater. 188, 2020, 192-202.
[4] D. Schliephake et al., Mechanical behavior at elevated temperatures of an Al-Mn-Mg-Sc-Zr alloy manufactured by selective laser melting, Mater. Sci. Eng. A 831, 2022, 142032.

Abstract

Abstract

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