Helmholtz Zentrum Berlin für Materialien und Energie GmbH
Technical
parts and components often have a highly inhomogeneous surface
topography in form of notches, grooves or strong local curvatures
(e.g. gear wheels, springs), which place very high demands on X-ray
stress analysis (XSA).
Since
XSA is based on the precise measurement of diffraction line positions
and their shifts due to the material inherent (i.e. residual)
stresses [1,2],
the surface topography of the investigated sample plays an important
role for measurements performed in reflection geometry. This is
because the depth range below the surface, from which the information
of the diffraction signal originates, is limited to a few tens to a
few hundred micrometers, depending on the photon energy and
absorption of the material. In [3] the authors have identified four
effects that cause diffraction line shifts in such cases and must
therefore be taken into account in the evaluation. The shifts
originate from
(i)
the rotation of the local stress reference system, (ii) its
translation from the diffractometer center, (iii) absorption and (iv)
partial shadowing and/or screening of the X-ray beam.
The
work presented aims at a systematic study of the rotation effect
(psi-missetting)
[4] by XSA using energy and angle dispersive diffraction performed on
a ferritic steel sample with a well-defined
surface
topography.
It is characterized by three grooves that have the same nominal
diameter but have been milled to different depths into the flat
surface. Modifications
of the fundamental equation of XSA are proposed that allow to correct
the hoop and longitudinal stresses obtained from sin2psi-measurements
on
samples featuring an inhomogeneous surface topography.
References
[1]
I.
C. Noyan, J. B. Cohen; Residual Stress Measurement by Diffraction and
Interpretation, New
York: Springer 1987.
[2]
V. Hauk;
Structural and Residual Stress Analysis by Nondestructive Methods,
Amsterdam: Elsevier 1997.
[3]
M. Francois,
J. M. Sprauel, J. L. Lebrun; in Proc. 3rd International Conference on
Residual Stresses (ICRS3), Tokushima, Japan, CRC Press 1992,
pp. 933 – 938.
[4]
M.
Francois, B. Dionnet, J. M. Sprauel, F. Nardou; J. Appl. Cryst. 1995
28, pp. 761 - 767.
Abstract
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