FEMS EUROMAT 2023
Poster
How Deep Does It Go: Revealing 3DStrains in Additively Manufactured Alloys
CY

Dr. Can Yildirim

European Synchrotron Radiation Facility - ESRF

Chen, Y.¹; Tang, Y.²; Collins, D.³; Clark, S.⁴; Ludwig, W.⁵; Rodriguez-Lamas, R.⁵; Detlefs, C.⁵; Reed, R.²; Lee, P.⁶; Withers, P.⁷; Yildirim, C. (Speaker)⁵
¹RMIT, Melbourne (Australia); ²University of Oxford, Oxfordshire (United Kingdom); ³University of Birmingham; ⁴Advanced Photon Source, Lemont (United States); ⁵European Synchrotron Radiation Facility, Grenoble (France); ⁶University College London; ⁷University of Manchester

Undesirable microstructures and high residual stresses in Laser Additive Manufacturing (LAM) present challenges due to rapid and complex solidification. Non-destructive assessment of mechanical performance and deformation patterning is crucial. Using Dark Field X-ray Microscopy (DFXM), we map 3D subsurface intragranular orientation and strain variations in a surface-breaking grain of a directed energy deposition nickel superalloy. DFXM reveals a highly heterogeneous 3D microstructure with <0.5° local orientation differences and lattice strain up to 0.005. The grain comprises ≈ 5 μm-sized cells with alternating strain states. DFXM results are compared to Electron Backscatter Diffraction measurements from the same grain's cut-off surface. We discuss microstructure developments during LAM, rationalizing deformation patterning formation from extreme thermal gradients during processing and susceptibility to solute segregation.

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